hf6391964 |
2010-09-24 10:00 |
Practical Process Research & Development By Neal G. Anderson 354 pages Publisher: Academic Press; 1st edition (April 15, 2000) Language: English -10: 0120594757 IN-13: 978-0120594757 Practical Process Research & Development teaches how to anticipate and avoid problems associated with scale-up from the research lab or pilot plant to full production. The approach is pragmatic, with a minimum of theory and over 100 practical scale-up tips. Many tables and detailed reaction schemes allow the reader to identify critical processing steps quickly. Target Audience: Novice and experienced process chemists and chemical engineers; especially valuable for anyone entering process chemistry from a classical organic chemistry background; it is also a superb text for students of process chemistry. Table of Contents: Approaches to Process Devlopment Route Selection Reagent Selection Solvent Selection Running the Reaction Effects of Water In-Process Controls Optimizing the Reaction by Minimizing Impurities Optimizing Catalytic Reactions Work-up Tools for Purifying the Product: Column Chromatography, Crystallization, and Reslurrying Final Product Form and Impurity Considerations Vessels and Mixing Preparing for and Implementing the Scale-up Run Troubleshooting Chiral Synthesis Index
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